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1 article(s) from Wenzel, Marianne

Synthesis of highly active ETS-10-based titanosilicate for heterogeneously catalyzed transesterification of triglycerides

Muhammad A. Zaheer,
David Poppitz,
Khavar Feyzullayeva,
Marianne Wenzel,
Jörg Matysik,
Radomir Ljupkovic,
Aleksandra Zarubica,
Alexander A. Karavaev,
Andreas Pöppl,
Roger Gläser and
Muslim Dvoyashkin

Beilstein J. Nanotechnol. 2019, 10, 2039–2061, doi:10.3762/bjnano.10.200

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Figure 1: One of the polymorphs of the microporous ETS-10 consisting of TiO₆ octahedra and SiO₄ tetrahedra sh...

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Figure 2: X-ray diffractograms of the as-synthesized ETS-10 material (Na,K-ETS-10, top) and of the reference ...

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Figure 3: SEM micrographs of selected crystals representing different types of phases formed during the synth...

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Figure 4: Nitrogen adsorption (solid circles) and desorption (open circles) isotherms of the as-synthesized N...

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Figure 5: Hg intrusion data of the as-synthesized Na,K-ETS-10 material.

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Figure 6: TEM micrographs for the Na,K-ETS-10 material obtained with different magnifications demonstrating a...

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Figure 7: (A) XRD data of post-synthetically treated titanosilicates. The calculated crystallinity decreased ...

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Figure 8: SEM micrographs of the titanosilicates treated with H₂O₂ for 30, 45 and 60 min (P-ETS-10/30, P-ETS-...

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Figure 9: (A) Nitrogen adsorption and desorption isotherms of titanosilicates treated with H₂O₂ for 30 min (l...

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Figure 10: TEM images of the selected crystals of P-ETS-10/60 and C-P-ETS 10/60 demonstrating the presence of ...

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Figure 11: Differential thermal analysis of the Na,K-ETS-10 (red), P-ETS-10/60 (blue) and C-P-ETS-10/60 (green...

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Figure 12: Temperature-programmed desorption of NH₃ (A) and CO₂ (B) in Na,K-ETS-10 (red), P-ETS-10/60 (blue) a...

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Figure 13: The HPDEC (A) and CP (B) ²⁹Si MAS NMR spectra obtained for Na,K-ETS-10 (red), P-ETS-10/60 (blue) an...

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Figure 14: The EPR spectra measured with Na,K-ETS-10 (red), P-ETS-10/60 (blue) and C-P-ETS-10/60 (green) at 70...

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Figure 15: Variable temperature HP ¹²⁹Xe NMR spectra acquired on Na,K-ETS-10 (A, red), P-ETS-10/60 (B, blue) a...

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Figure 16: ¹H PFG NMR diffusion attenuation curves of bulk triolein (dashed line) and triolein in oversaturate...

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Figure 17: Schematic representation of the diffusion modes denoted as 1, 2 and 3 in the Figure 16 as observed by PFG NM...

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Figure 18: Conversion of triolein over CaO- (A) and ETS-10-based (B) catalysts at 403 K measured for different...

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Published 28 Oct 2019

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